MWexperimental | 997 | kDa |
MWexpected | 56 | kDa |
VPorod | 1820 | nm3 |
log I(s)
3.80×102
3.80×101
3.80×100
3.80×10-1
|
s, nm-1
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Synchrotron SAXS
data from solutions of
Metal-free hETHE1, 5 mg/ml
in
50 mM Tris 150 mM NaCl 2 mM TCEP, pH 8
were collected
on the
EMBL X33 beam line
at the DORIS III, DESY storage ring
(Hamburg, Germany)
using a Pilatus 1M-W detector
at a sample-detector distance of 2.7 m and
at a wavelength of λ = 0.15 nm
(I(s) vs s, where s = 4πsinθ/λ, and 2θ is the scattering angle).
One solute concentration of 5.00 mg/ml was measured
at 5°C.
30 successive
frames were collected.
The data were normalized to the intensity of the transmitted beam and radially averaged; the scattering of the solvent-blank was subtracted.
Storage temperature = UNKNOWN. X-ray Exposure time = UNKNOWN
Tags:
X33
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